Synthesis and characterization of metallic complexes of 3-(2-furyl) 2-propenal semicarbazone with d element dihalides
Identifieur interne : 000F17 ( Main/Exploration ); précédent : 000F16; suivant : 000F18Synthesis and characterization of metallic complexes of 3-(2-furyl) 2-propenal semicarbazone with d element dihalides
Auteurs : G. Ibrahim [France] ; M. A. Khan [France] ; P. Richomme [France] ; O. Benali-Baïtich [Algérie] ; G. Bouet [France]Source :
- Polyhedron [ 0277-5387 ] ; 1997.
Abstract
3-(2-Furyl) 2-propenal semicarbazone (FASC) and CoII, NiII, CuII, ZnII and CdII chlorides or bromides gave the complexes: [M(FASC)2X2], [M(FASC)2]X2 or [M(FASC)X2] which were characterized starting from elemental analysis and molar conductances. Their structures are discussed on the basis of magnetic moments, infrared and electronic spectra; in addition, the NMR data are used in the case of ZnII and CdII species. The main cell parameters are given using X-ray diffraction powder diagrams.
Url:
DOI: 10.1016/S0277-5387(97)00063-6
Affiliations:
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<front><div type="abstract" xml:lang="en">3-(2-Furyl) 2-propenal semicarbazone (FASC) and CoII, NiII, CuII, ZnII and CdII chlorides or bromides gave the complexes: [M(FASC)2X2], [M(FASC)2]X2 or [M(FASC)X2] which were characterized starting from elemental analysis and molar conductances. Their structures are discussed on the basis of magnetic moments, infrared and electronic spectra; in addition, the NMR data are used in the case of ZnII and CdII species. The main cell parameters are given using X-ray diffraction powder diagrams.</div>
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